[1]王自梁,王景迪,邹依霖,等.川芎与东川芎挥发性成分分析[J].延边大学学报(自然科学版),2016,42(03):217-220.
　WANG Ziliang,WANG Jingdi,ZOU Yilin,et al.Analysis of the volatile component from Ligusticum chuanxiong Hort. and Cnidium officinale Makino[J].Journal of Yanbian University,2016,42(03):217-220.
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川芎与东川芎挥发性成分分析

《延边大学学报(自然科学版)》[ISSN:1004-4353/CN:22-1191/N] 卷: 第42卷 期数: 2016年03期 页码: 217-220 栏目: 应用科学研究 出版日期: 2016-07-20
Title:
Analysis of the volatile component from Ligusticum chuanxiong Hort. and Cnidium officinale Makino
作者:
王自梁1;  王景迪1;  邹依霖2;  安仁波1; 2
1.延边大学药学院, 吉林 延吉 133002; 2.延边大学长白山生物资源与功能分子教育部重点实验室, 吉林 延吉 133002
Author(s):
WANG Ziliang1;  WANG Jingdi1;  ZOU Yilin2;  AN Renbo1; 2
1.College of Pharmacy, Yanbian University, Yanji 133002, China; 2.Key Laboratory of Natural Resources of Changbai Mountain & Functional Molecules (Yanbian University), Ministry of Education, Yanji 133002, China
关键词:
川芎;  东川芎;  挥发性成分;  2-羟基-苯乙酸异丁酯;  气流吹扫-微注射器萃取技术;  气相色谱-质谱仪
Keywords:
Ligusticum chuanxiong Hort.;  Cnidium officinale Makino;  the volatile component;  isobutyl 2-(2-hydroxyphenyl)acetate;  gas purge microsyringe extraction;  gas chromatograph-mass spectrometer
分类号:
R284.1
文献标志码:
A
摘要:
用气流吹扫-微注射器萃取技术(GP-MSE)得到川芎和东川芎的挥发性成分,用气相色谱-质谱联用(GC-MS)鉴定了所得挥发性物质的化学成分,并用归一化法测定了其相对含量.在川芎中鉴定出2-羟基-苯乙酸异丁酯(21.94%)、间苯二胺(6.04%)、丁烯苯酞(5.17%)和1-(2,4-二甲基苯基)-2-甲基-1-丙酮(4.83%)等32个化合物.在东川芎中鉴定出(1Z,4Z)-6-丁基环庚-1,4-二烯(15.76%)、2-羟基-苯乙酸异丁酯(13.46%)、(11E,14E)-二十碳二烯酸甲酯(9.32%)和1-(2,4-二甲基苯基)-1-丙酮(5.61%)等34个化合物.2-羟基-苯乙酸异丁酯为首次从川芎和东川芎中鉴定出的成分,其相对百分含量分别为21.94%和13.46%.
Abstract:
The volatile component of Ligusticum chuanxiong Hort. and Cnidium officinale Makino were handled by gas purge microsyringe extraction(GP-MSE), and were analyzed by gas chromatograph-mass spectrometer(GC-MS). Area normalization method was used for the detection of the volatile component. Thirty-two compounds were identified from Ligusticum chuanxiong Hort. and the components conclude isobutyl 2-(2-hydroxyphenyl)acetate(21.94%), benzene-1,3-diamine(6.04%), n -butene phthalide(5.17%), 1-(2,4-dimethylphenyl)-2-methylpropan -1-one(4.83%), etc; thirty-four compounds were extracted and identified from Cnidium officinale Makino, the components conclude(1Z,4Z)-6-butylcyclohepta-1,4-diene(15.76%), isobutyl 2-(2-hydroxyphenyl)acetate(13.46%),(11E,14E)-methyl icosa-11,14-dienoate(9.32%), 1-(2,4-dimethylphenyl)propan-1-one(5.61%), etc. The component isobutyl 2-(2-hydroxyphenyl)acetate was identified from Ligusticum chuanxiong Hort. and Cnidium officinale Makino for the first time,the relative percentage content is 21.94% and 13.46%, respectively.

参考文献/References:

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备注/Memo

收稿日期: 2016-07-29 基金项目: 吉林省科学技术厅项目(20130102077JC)*通信作者: 安仁波(1965—),男,博士,教授,研究方向为天然药物活性成分.

更新日期/Last Update: 2016-10-20